Macroscale and Microscale Organic Experiments 6th Edition by Kenneth L. Williamson and Katherine M. Masters derives many experiments and procedures from the traditional Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content.
The book contains new experiments that stress greener chemistry, up to date NMR spectra, and a Premium site that includes glassware-particular movies with pre-lab exercises. Providing a versatile mixture of macroscale and microscale choices for most experiments, this proven handbook permits customers to save on the acquisition and disposal of pricy, generally hazardous organic chemicals.
Macroscale versions can be used for less costly experiments, giving readers experience working with conventionally sized glassware. There are experiments that stress greener chemistry seem throughout the manual and are recognized with a green chemistry icon. For instance, using household bleach is explored as an alternative choice to the toxic chromium ion as an oxidizing agent for cyclohexanol.
The laboratory security chapter contains material on working with closed programs and laboratory courtesy. The chapter on mass spectrometry describes time-of-flight and mass quadrupole analyzers and includes sections on GC-MS and computer-aided spectral identification, in addition to ESI and MALDI ionization. The manual's bioassay experiments embody a bioassay of eugenol isolated from cloves.
Material is obtainable on diffuse reflectance IR analysis, capillary GC, and temperature programming. The chapter on mass spectrometry describes time-of-flight and mass quadrupole analyzers and includes sections on GC-MS and computer-aided spectral identification as well as ESI and MALDI ionization. Bioassay experiments embrace a bioassay of eugenol isolated from cloves. Material is obtainable on diffuse reflectance IR analysis, capillary GC, and temperature programming.
The place of natural chemistry labwork has been put in a broader context via reorganization and revisions to the primary fifteen chapters dealing with basic lab methods, computational chemistry, and instrumental methods. Computational chemistry, which allows college students to find out the precise construction of molecules, supplies prolonged coverage of ab initio and semi-empirical models and calculations.
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